A new method of obtaining sorbent studied its sorption capacity with respect to the studied ions. Identified and studied the parameters of complex sorption of pollutants from the wastewater of food businesses. It is shown that the value of Maximalno achievable efficiency concentrating the extraction of ions in the co-precipitation of sorbent on the order exceeds the corresponding values that characterize sorption on other sorbents. Selection sorbent used to concentrate metal ions from process effluent complex composition.